BMRB Entry 20105
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20105
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Title: BI-32169 PubMed: 20043911
Deposition date: 2009-10-20 Original release date: 2010-01-06
Authors: Knappe, Thomas A.; Linne, Uwe; Xie, Xiulan; Marahiel, Mohamed A.
Citation: Knappe, Thomas; Linne, Uwe; Xie, Xiulan; Marahiel, Mohamed. "The glucagon receptor antagonist BI-32169 constitutes a new class of lasso peptides." FEBS Lett. 584, 785-789 (2010).
Assembly members:
BI-32169, polymer, 19 residues, Formula weight is not available
Natural source: Common Name: Streptomyces sp. Taxonomy ID: 1931 Superkingdom: Eubacteria Kingdom: not available Genus/species: Streptomyces Streptomyces sp.
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
BI-32169: GLPWGCPSDIPGWNTPWAC
- assigned_chemical_shifts
- conformer_family_coord_set
Data type | Count |
1H chemical shifts | 108 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | BI | 1 |
Entities:
Entity 1, BI 19 residues - Formula weight is not available
1 | GLY | LEU | PRO | TRP | GLY | CYS | PRO | SER | ASP | ILE | ||||
2 | PRO | GLY | TRP | ASN | THR | PRO | TRP | ALA | CYS |
Samples:
sample_1: BI-321693 5 mM
sample_conditions_1: pH: .; temperature: 313 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA v2.1, Goddard, Guntert, Mumenthaler and Wuthrich, Tripos - chemical shift assignment, geometry optimization, structure solution
NMR spectrometers:
- Bruker Avance 600 MHz
Related Database Links:
PDB |