BMRB Entry 20128
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20128
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Title: solution structure of conotoxin qc16a
Deposition date: 2011-01-16 Original release date: 2011-07-08
Authors: Hong, Jing; Lin, Donghai
Citation: Hong, Jing; Lin, Donghai. "Solution structure of conotoxin qc16a" . ., .-..
Assembly members:
conotoxin_qc16a, polymer, 11 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
conotoxin_qc16a: DCQPCGHNVCC
- assigned_chemical_shifts
Data type | Count |
1H chemical shifts | 47 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | conotoxin qc16a | 1 |
Entities:
Entity 1, conotoxin qc16a 11 residues - Formula weight is not available
1 | ASP | CYS | GLN | PRO | CYS | GLY | HIS | ASN | VAL | CYS | ||||
2 | CYS |
Samples:
sample_1: conotoxin qc16a 4 mM; H2O 90%; D2O 10%
sample_2: conotoxin qc16a 4 mM; D2O 100%
sample_conditions_1: pH: 3.5; temperature: 298 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H TOCSY no.1 | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY no.1 | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H TOCSY no.2 | sample_2 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY no.2 | sample_2 | isotropic | sample_conditions_1 |
Software:
SPARKY v3.11, Goddard - chemical shift assignment
ARIA v2.2, Linge, O, . - chemical shift assignment
CNS v1.1, Brunger, Adams, Clore, Gros, Nilges and Read - structure solution
NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
NMR spectrometers:
- Varian INOVA 600 MHz