BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
Member of WWPDB

BMRB Entry 19580

Title: PAP262-270 in SDS micelles

Deposition date: 2013-10-24 Original release date: 2014-10-27

Authors: Blokhin, Dmitriy; Vklochkov, Vladimir; Filippov, Andrey; Antzutkin, Oleg

Citation: Blokhin, Dmitriy. "PAP262-270 in SDS micelles"  Not known ., .-..

Assembly members:
entity_1, polymer, 11 residues, 1051.228 Da.

Natural source:   Common Name: Human   Taxonomy ID: 9606   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Homo sapiens

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):
entity_1: XVLVNEILNHX

Data sets:
Data typeCount
1H chemical shifts80

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1PAP262-270 in SDS micelles1

Entities:

Entity 1, PAP262-270 in SDS micelles 11 residues - 1051.228 Da.

1   ACEVALLEUVALASNGLUILELEUASNHIS
2   NH2

Samples:

sample_1: PAP262-270 300 uM; SDS 50 mM; H2O 90%; D2O 10%

sample_conditions_1: temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

X-PLOR NIH, Schwieters, Kuszewski, Tjandra and Clore - structure solution

SPARKY, Goddard - chemical shift assignment

NMR spectrometers:

  • Bruker Avance 500 MHz