BMRB Entry 21002
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21002
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Title: Solution NMR structure of TZ2C-BG PubMed: 21989967
Deposition date: 2011-03-11 Original release date: 2012-08-07
Authors: McElheny, Dan; Keiderling, Timothy
Citation: Wu, Ling; McElheny, Dan; Setnicka, Vladimir; Hilario, Jovencio; Keiderling, Timothy. "Role of different beta-turns in beta-hairpin conformation and stability studied by optical spectroscopy" . 80, 44-60 (2012).
Assembly members:
TrpZip2c-BG, polymer, 13 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
TrpZip2c-BG: AWAWEXGKWAWKX
- assigned_chemical_shifts
- coupling_constants
Data type | Count |
1H chemical shifts | 87 |
coupling constants | 10 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | TrpZip2c-BG | 1 |
Entities:
Entity 1, TrpZip2c-BG 13 residues - Formula weight is not available
1 | ALA | TRP | ALA | TRP | GLU | AIB | GLY | LYS | TRP | ALA | ||||
2 | TRP | LYS | NH2 |
Samples:
sample_1: TrpZip2c-BG4 4.1 mM; sodium phosphate 20 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 0.02 M; pH: 5.8; pressure: 1 atm; temperature: 283 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H COSY | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA v2.0, Guntert, Mumenthaler and Wuthrich - structure solution
NMR spectrometers:
- Bruker Avance 800 MHz