data_6485 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 6485 _Entry.Title ; A novel RNA pentaloop fold involved in targeting ADAR2 ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2005-02-03 _Entry.Accession_date 2005-02-04 _Entry.Last_release_date . _Entry.Original_release_date . _Entry.Origination author _Entry.NMR_STAR_version 3.1.1.61 _Entry.Original_NMR_STAR_version 2.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.Entry_ID 1 Richard Stefl . . . 6485 2 Frederic Allain . . . 6485 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 6485 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 183 6485 '1H chemical shifts' 221 6485 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2011-04-20 2011-04-07 update author 'Update chemical shifts' 6485 1 . . 2005-05-26 2005-02-03 original author 'Original release' 6485 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 6485 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 15840813 _Citation.Full_citation . _Citation.Title 'A novel RNA pentaloop fold involved in targeting ADAR2' _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev RNA _Citation.Journal_name_full . _Citation.Journal_volume 11 _Citation.Journal_issue 5 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 592 _Citation.Page_last 597 _Citation.Year 2005 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.Entry_ID _Citation_author.Citation_ID 1 R. Stefl . . . 6485 1 2 F. Allain . H. . 6485 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_GluR-B_R_G_RNA _Assembly.Sf_category assembly _Assembly.Sf_framecode GluR-B_R_G_RNA _Assembly.Entry_ID 6485 _Assembly.ID 1 _Assembly.Name 'GluR-B R/G RNA' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state 'not present' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Assembly_type.Type _Assembly_type.Entry_ID _Assembly_type.Assembly_ID monomer 6485 1 stop_ loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'GluR-B R/G RNA' 1 $R_G_stem-loop . . . native . . . . . 6485 1 stop_ loop_ _Assembly_common_name.Name _Assembly_common_name.Type _Assembly_common_name.Entry_ID _Assembly_common_name.Assembly_ID 'GluR-B R/G RNA' abbreviation 6485 1 'GluR-B R/G RNA' system 6485 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_R_G_stem-loop _Entity.Sf_category entity _Entity.Sf_framecode R_G_stem-loop _Entity.Entry_ID 6485 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'GluR-B R/G stem-loop RNA' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GGUAACAAUAUGCUAAAUGU UGUUACC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer . _Entity.Nstd_chirality . _Entity.Nstd_linkage . _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 27 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic . _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_common_name.Name _Entity_common_name.Type _Entity_common_name.Entry_ID _Entity_common_name.Entity_ID 'GluR-B R/G stem-loop RNA' common 6485 1 'R/G stem-loop' abbreviation 6485 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . G . 6485 1 2 . G . 6485 1 3 . U . 6485 1 4 . A . 6485 1 5 . A . 6485 1 6 . C . 6485 1 7 . A . 6485 1 8 . A . 6485 1 9 . U . 6485 1 10 . A . 6485 1 11 . U . 6485 1 12 . G . 6485 1 13 . C . 6485 1 14 . U . 6485 1 15 . A . 6485 1 16 . A . 6485 1 17 . A . 6485 1 18 . U . 6485 1 19 . G . 6485 1 20 . U . 6485 1 21 . U . 6485 1 22 . G . 6485 1 23 . U . 6485 1 24 . U . 6485 1 25 . A . 6485 1 26 . C . 6485 1 27 . C . 6485 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 6485 1 . G 2 2 6485 1 . U 3 3 6485 1 . A 4 4 6485 1 . A 5 5 6485 1 . C 6 6 6485 1 . A 7 7 6485 1 . A 8 8 6485 1 . U 9 9 6485 1 . A 10 10 6485 1 . U 11 11 6485 1 . G 12 12 6485 1 . C 13 13 6485 1 . U 14 14 6485 1 . A 15 15 6485 1 . A 16 16 6485 1 . A 17 17 6485 1 . U 18 18 6485 1 . G 19 19 6485 1 . U 20 20 6485 1 . U 21 21 6485 1 . G 22 22 6485 1 . U 23 23 6485 1 . U 24 24 6485 1 . A 25 25 6485 1 . C 26 26 6485 1 . C 27 27 6485 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 6485 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Subvariant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Cellular_location _Entity_natural_src.Fragment _Entity_natural_src.Fraction _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Plasmid_details _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Dev_stage _Entity_natural_src.Details _Entity_natural_src.Citation_ID _Entity_natural_src.Citation_label _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $R_G_stem-loop . Human organism . 'Homo sapiens' 9606 . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . . . . . . . . . 6485 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 6485 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_subvariant _Entity_experimental_src.Host_org_organ _Entity_experimental_src.Host_org_tissue _Entity_experimental_src.Host_org_tissue_fraction _Entity_experimental_src.Host_org_cell_line _Entity_experimental_src.Host_org_cell_type _Entity_experimental_src.Host_org_cellular_location _Entity_experimental_src.Host_org_organelle _Entity_experimental_src.Host_org_gene _Entity_experimental_src.Host_org_culture_collection _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Host_org_dev_stage _Entity_experimental_src.Details _Entity_experimental_src.Citation_ID _Entity_experimental_src.Citation_label _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $R_G_stem-loop . 'cell free synthesis' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6485 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 6485 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'GluR-B R/G stem-loop RNA' '[U-13C; U-15N]' . . 1 $R_G_stem-loop . . . 0.5 2 mM . . . . 6485 1 stop_ save_ ####################### # Sample conditions # ####################### save_condition_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode condition_1 _Sample_condition_list.Entry_ID 6485 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6 0.1 pH 6485 1 temperature 303 1 K 6485 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 6485 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 900 save_ save_NMR_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_2 _NMR_spectrometer.Entry_ID 6485 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode spectrometer_list _NMR_spectrometer_list.Entry_ID 6485 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Bruker Avance . 900 . . . 6485 1 2 NMR_spectrometer_2 Bruker Avance . 600 . . . 6485 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 6485 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D NOESY' . . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . . . . . . . . . . . . . . . . . . . 6485 1 2 '2D TOCSY' . . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . . . . . . . . . . . . . . . . . . . 6485 1 3 13C-HSQC . . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . . . . . . . . . . . . . . . . . . . 6485 1 4 '3D 13-separated NOESY' . . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . . . . . . . . . . . . . . . . . . . 6485 1 5 'and 3D HCCH-TOCSY' . . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . . . . . . . . . . . . . . . . . . . 6485 1 stop_ save_ save_NMR_spec_expt__0_1 _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode NMR_spec_expt__0_1 _NMR_spec_expt.Entry_ID 6485 _NMR_spec_expt.ID 1 _NMR_spec_expt.Name '2D NOESY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID . _NMR_spec_expt.NMR_spectrometer_label . _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_NMR_spec_expt__0_2 _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode NMR_spec_expt__0_2 _NMR_spec_expt.Entry_ID 6485 _NMR_spec_expt.ID 2 _NMR_spec_expt.Name '2D TOCSY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID . _NMR_spec_expt.NMR_spectrometer_label . _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_NMR_spec_expt__0_3 _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode NMR_spec_expt__0_3 _NMR_spec_expt.Entry_ID 6485 _NMR_spec_expt.ID 3 _NMR_spec_expt.Name 13C-HSQC _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID . _NMR_spec_expt.NMR_spectrometer_label . _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_NMR_spec_expt__0_4 _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode NMR_spec_expt__0_4 _NMR_spec_expt.Entry_ID 6485 _NMR_spec_expt.ID 4 _NMR_spec_expt.Name '3D 13-separated NOESY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID . _NMR_spec_expt.NMR_spectrometer_label . _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_NMR_spec_expt__0_5 _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode NMR_spec_expt__0_5 _NMR_spec_expt.Entry_ID 6485 _NMR_spec_expt.ID 5 _NMR_spec_expt.Name 'and 3D HCCH-TOCSY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID . _NMR_spec_expt.NMR_spectrometer_label . _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference _Chem_shift_reference.Entry_ID 6485 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Indirect_shift_ratio_cit_ID _Chem_shift_ref.Indirect_shift_ratio_cit_label _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Correction_val_cit_ID _Chem_shift_ref.Correction_val_cit_label _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 DSS 'methyl protons' . . . . ppm 0.0 . indirect 0.251449530 . . . 1 $entry_citation . . 1 $entry_citation 6485 1 H 1 DSS 'methyl protons' . . . . ppm 0.0 internal direct 1.0 . . . 1 $entry_citation . . 1 $entry_citation 6485 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_shift_set_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_1 _Assigned_chem_shift_list.Entry_ID 6485 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $condition_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 6485 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 G H8 H 1 8.14 . . 1 . . . . . . . . 6485 1 2 . 1 1 1 1 G C8 C 13 139.3 . . 1 . . . . . . . . 6485 1 3 . 1 1 1 1 G H1' H 1 5.81 . . 1 . . . . . . . . 6485 1 4 . 1 1 1 1 G H2' H 1 4.95 . . 1 . . . . . . . . 6485 1 5 . 1 1 1 1 G H3' H 1 4.7 . . 1 . . . . . . . . 6485 1 6 . 1 1 1 1 G H4' H 1 4.55 . . 1 . . . . . . . . 6485 1 7 . 1 1 1 1 G H5' H 1 4.24 . . 2 . . . . . . . . 6485 1 8 . 1 1 1 1 G H5'' H 1 4.42 . . 2 . . . . . . . . 6485 1 9 . 1 1 1 1 G C1' C 13 92.1 . . 1 . . . . . . . . 6485 1 10 . 1 1 1 1 G C2' C 13 75.1 . . 1 . . . . . . . . 6485 1 11 . 1 1 1 1 G C3' C 13 74.5 . . 1 . . . . . . . . 6485 1 12 . 1 1 1 1 G C4' C 13 83.6 . . 1 . . . . . . . . 6485 1 13 . 1 1 1 1 G C5' C 13 67.2 . . 1 . . . . . . . . 6485 1 14 . 1 1 2 2 G H1 H 1 13.32 . . 1 . . . . . . . . 6485 1 15 . 1 1 2 2 G H8 H 1 7.53 . . 1 . . . . . . . . 6485 1 16 . 1 1 2 2 G C8 C 13 137 . . 1 . . . . . . . . 6485 1 17 . 1 1 2 2 G H1' H 1 5.89 . . 1 . . . . . . . . 6485 1 18 . 1 1 2 2 G H2' H 1 4.53 . . 1 . . . . . . . . 6485 1 19 . 1 1 2 2 G H3' H 1 4.53 . . 1 . . . . . . . . 6485 1 20 . 1 1 2 2 G H4' H 1 4.54 . . 1 . . . . . . . . 6485 1 21 . 1 1 2 2 G H5' H 1 4.22 . . 2 . . . . . . . . 6485 1 22 . 1 1 2 2 G H5'' H 1 4.50 . . 2 . . . . . . . . 6485 1 23 . 1 1 2 2 G C1' C 13 93.3 . . 1 . . . . . . . . 6485 1 24 . 1 1 2 2 G C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 25 . 1 1 2 2 G C3' C 13 73.1 . . 1 . . . . . . . . 6485 1 26 . 1 1 2 2 G C4' C 13 82.7 . . 1 . . . . . . . . 6485 1 27 . 1 1 2 2 G C5' C 13 66.1 . . 1 . . . . . . . . 6485 1 28 . 1 1 3 3 U H3 H 1 13.52 . . 1 . . . . . . . . 6485 1 29 . 1 1 3 3 U H5 H 1 5.14 . . 1 . . . . . . . . 6485 1 30 . 1 1 3 3 U H6 H 1 7.75 . . 1 . . . . . . . . 6485 1 31 . 1 1 3 3 U C5 C 13 103.2 . . 1 . . . . . . . . 6485 1 32 . 1 1 3 3 U C6 C 13 141.4 . . 1 . . . . . . . . 6485 1 33 . 1 1 3 3 U H1' H 1 5.52 . . 1 . . . . . . . . 6485 1 34 . 1 1 3 3 U H2' H 1 4.56 . . 1 . . . . . . . . 6485 1 35 . 1 1 3 3 U H3' H 1 4.58 . . 1 . . . . . . . . 6485 1 36 . 1 1 3 3 U H4' H 1 4.45 . . 1 . . . . . . . . 6485 1 37 . 1 1 3 3 U H5' H 1 4.11 . . 2 . . . . . . . . 6485 1 38 . 1 1 3 3 U H5'' H 1 4.58 . . 2 . . . . . . . . 6485 1 39 . 1 1 3 3 U C1' C 13 93.8 . . 1 . . . . . . . . 6485 1 40 . 1 1 3 3 U C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 41 . 1 1 3 3 U C3' C 13 72.4 . . 1 . . . . . . . . 6485 1 42 . 1 1 3 3 U C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 43 . 1 1 3 3 U C5' C 13 64.6 . . 1 . . . . . . . . 6485 1 44 . 1 1 4 4 A H2 H 1 6.40 . . 1 . . . . . . . . 6485 1 45 . 1 1 4 4 A H8 H 1 8.06 . . 1 . . . . . . . . 6485 1 46 . 1 1 4 4 A C2 C 13 152.3 . . 1 . . . . . . . . 6485 1 47 . 1 1 4 4 A C8 C 13 139.7 . . 1 . . . . . . . . 6485 1 48 . 1 1 4 4 A H1' H 1 5.9 . . 1 . . . . . . . . 6485 1 49 . 1 1 4 4 A H2' H 1 4.54 . . 1 . . . . . . . . 6485 1 50 . 1 1 4 4 A H3' H 1 4.71 . . 1 . . . . . . . . 6485 1 51 . 1 1 4 4 A H4' H 1 4.53 . . 1 . . . . . . . . 6485 1 52 . 1 1 4 4 A H5' H 1 4.19 . . 2 . . . . . . . . 6485 1 53 . 1 1 4 4 A H5'' H 1 4.53 . . 2 . . . . . . . . 6485 1 54 . 1 1 4 4 A C1' C 13 92.9 . . 1 . . . . . . . . 6485 1 55 . 1 1 4 4 A C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 56 . 1 1 4 4 A C3' C 13 73.4 . . 1 . . . . . . . . 6485 1 57 . 1 1 4 4 A C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 58 . 1 1 4 4 A C5' C 13 65.9 . . 1 . . . . . . . . 6485 1 59 . 1 1 5 5 A H2 H 1 7.55 . . 1 . . . . . . . . 6485 1 60 . 1 1 5 5 A H8 H 1 7.83 . . 1 . . . . . . . . 6485 1 61 . 1 1 5 5 A C2 C 13 153.9 . . 1 . . . . . . . . 6485 1 62 . 1 1 5 5 A C8 C 13 139.1 . . 1 . . . . . . . . 6485 1 63 . 1 1 5 5 A H1' H 1 5.81 . . 1 . . . . . . . . 6485 1 64 . 1 1 5 5 A H2' H 1 4.41 . . 1 . . . . . . . . 6485 1 65 . 1 1 5 5 A H3' H 1 4.56 . . 1 . . . . . . . . 6485 1 66 . 1 1 5 5 A H4' H 1 4.47 . . 1 . . . . . . . . 6485 1 67 . 1 1 5 5 A H5' H 1 4.14 . . 2 . . . . . . . . 6485 1 68 . 1 1 5 5 A H5'' H 1 4.58 . . 2 . . . . . . . . 6485 1 69 . 1 1 5 5 A C1' C 13 92.7 . . 1 . . . . . . . . 6485 1 70 . 1 1 5 5 A C2' C 13 75.7 . . 1 . . . . . . . . 6485 1 71 . 1 1 5 5 A C3' C 13 72.8 . . 1 . . . . . . . . 6485 1 72 . 1 1 5 5 A C4' C 13 82.2 . . 1 . . . . . . . . 6485 1 73 . 1 1 5 5 A C5' C 13 65.3 . . 1 . . . . . . . . 6485 1 74 . 1 1 6 6 C H5 H 1 5.15 . . 1 . . . . . . . . 6485 1 75 . 1 1 6 6 C H6 H 1 7.38 . . 1 . . . . . . . . 6485 1 76 . 1 1 6 6 C C5 C 13 97.7 . . 1 . . . . . . . . 6485 1 77 . 1 1 6 6 C C6 C 13 140.2 . . 1 . . . . . . . . 6485 1 78 . 1 1 6 6 C H1' H 1 5.25 . . 1 . . . . . . . . 6485 1 79 . 1 1 6 6 C H2' H 1 4.31 . . 1 . . . . . . . . 6485 1 80 . 1 1 6 6 C H3' H 1 4.41 . . 1 . . . . . . . . 6485 1 81 . 1 1 6 6 C H4' H 1 4.35 . . 1 . . . . . . . . 6485 1 82 . 1 1 6 6 C H5' H 1 4.04 . . 2 . . . . . . . . 6485 1 83 . 1 1 6 6 C H5'' H 1 4.48 . . 2 . . . . . . . . 6485 1 84 . 1 1 6 6 C C1' C 13 93.6 . . 1 . . . . . . . . 6485 1 85 . 1 1 6 6 C C2' C 13 75.6 . . 1 . . . . . . . . 6485 1 86 . 1 1 6 6 C C3' C 13 72.4 . . 1 . . . . . . . . 6485 1 87 . 1 1 6 6 C C4' C 13 81.8 . . 1 . . . . . . . . 6485 1 88 . 1 1 6 6 C C5' C 13 64.8 . . 1 . . . . . . . . 6485 1 89 . 1 1 7 7 A H2 H 1 6.74 . . 1 . . . . . . . . 6485 1 90 . 1 1 7 7 A H8 H 1 7.90 . . 1 . . . . . . . . 6485 1 91 . 1 1 7 7 A C2 C 13 152.4 . . 1 . . . . . . . . 6485 1 92 . 1 1 7 7 A C8 C 13 139.6 . . 1 . . . . . . . . 6485 1 93 . 1 1 7 7 A H1' H 1 5.83 . . 1 . . . . . . . . 6485 1 94 . 1 1 7 7 A H2' H 1 4.64 . . 1 . . . . . . . . 6485 1 95 . 1 1 7 7 A H3' H 1 4.41 . . 1 . . . . . . . . 6485 1 96 . 1 1 7 7 A H4' H 1 4.48 . . 1 . . . . . . . . 6485 1 97 . 1 1 7 7 A H5' H 1 4.12 . . 2 . . . . . . . . 6485 1 98 . 1 1 7 7 A H5'' H 1 4.51 . . 2 . . . . . . . . 6485 1 99 . 1 1 7 7 A C1' C 13 93.0 . . 1 . . . . . . . . 6485 1 100 . 1 1 7 7 A C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 101 . 1 1 7 7 A C3' C 13 72.7 . . 1 . . . . . . . . 6485 1 102 . 1 1 7 7 A C4' C 13 82.2 . . 1 . . . . . . . . 6485 1 103 . 1 1 7 7 A C5' C 13 65.4 . . 1 . . . . . . . . 6485 1 104 . 1 1 8 8 A H2 H 1 7.70 . . 1 . . . . . . . . 6485 1 105 . 1 1 8 8 A H8 H 1 7.64 . . 1 . . . . . . . . 6485 1 106 . 1 1 8 8 A C2 C 13 154 . . 1 . . . . . . . . 6485 1 107 . 1 1 8 8 A C8 C 13 139.1 . . 1 . . . . . . . . 6485 1 108 . 1 1 8 8 A H1' H 1 5.83 . . 1 . . . . . . . . 6485 1 109 . 1 1 8 8 A H2' H 1 4.55 . . 1 . . . . . . . . 6485 1 110 . 1 1 8 8 A H3' H 1 4.68 . . 1 . . . . . . . . 6485 1 111 . 1 1 8 8 A H4' H 1 4.48 . . 1 . . . . . . . . 6485 1 112 . 1 1 8 8 A H5' H 1 4.10 . . 2 . . . . . . . . 6485 1 113 . 1 1 8 8 A H5'' H 1 4.53 . . 2 . . . . . . . . 6485 1 114 . 1 1 8 8 A C1' C 13 93.2 . . 1 . . . . . . . . 6485 1 115 . 1 1 8 8 A C2' C 13 75.6 . . 1 . . . . . . . . 6485 1 116 . 1 1 8 8 A C3' C 13 73.2 . . 1 . . . . . . . . 6485 1 117 . 1 1 8 8 A C4' C 13 82.2 . . 1 . . . . . . . . 6485 1 118 . 1 1 8 8 A C5' C 13 65.3 . . 1 . . . . . . . . 6485 1 119 . 1 1 9 9 U H3 H 1 11.58 . . 1 . . . . . . . . 6485 1 120 . 1 1 9 9 U H5 H 1 5.32 . . 1 . . . . . . . . 6485 1 121 . 1 1 9 9 U H6 H 1 7.47 . . 1 . . . . . . . . 6485 1 122 . 1 1 9 9 U C5 C 13 104.4 . . 1 . . . . . . . . 6485 1 123 . 1 1 9 9 U C6 C 13 140.2 . . 1 . . . . . . . . 6485 1 124 . 1 1 9 9 U H1' H 1 5.22 . . 1 . . . . . . . . 6485 1 125 . 1 1 9 9 U H2' H 1 4.10 . . 1 . . . . . . . . 6485 1 126 . 1 1 9 9 U H3' H 1 4.51 . . 1 . . . . . . . . 6485 1 127 . 1 1 9 9 U H4' H 1 4.38 . . 1 . . . . . . . . 6485 1 128 . 1 1 9 9 U H5' H 1 4.06 . . 2 . . . . . . . . 6485 1 129 . 1 1 9 9 U H5'' H 1 4.47 . . 2 . . . . . . . . 6485 1 130 . 1 1 9 9 U C1' C 13 93.3 . . 1 . . . . . . . . 6485 1 131 . 1 1 9 9 U C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 132 . 1 1 9 9 U C3' C 13 72.8 . . 1 . . . . . . . . 6485 1 133 . 1 1 9 9 U C4' C 13 82.6 . . 1 . . . . . . . . 6485 1 134 . 1 1 9 9 U C5' C 13 64.5 . . 1 . . . . . . . . 6485 1 135 . 1 1 10 10 A H2 H 1 7.37 . . 1 . . . . . . . . 6485 1 136 . 1 1 10 10 A H8 H 1 8.28 . . 1 . . . . . . . . 6485 1 137 . 1 1 10 10 A C2 C 13 153.6 . . 1 . . . . . . . . 6485 1 138 . 1 1 10 10 A C8 C 13 140.9 . . 1 . . . . . . . . 6485 1 139 . 1 1 10 10 A H1' H 1 5.94 . . 1 . . . . . . . . 6485 1 140 . 1 1 10 10 A H2' H 1 4.47 . . 1 . . . . . . . . 6485 1 141 . 1 1 10 10 A H3' H 1 4.7 . . 1 . . . . . . . . 6485 1 142 . 1 1 10 10 A H4' H 1 4.45 . . 1 . . . . . . . . 6485 1 143 . 1 1 10 10 A H5' H 1 4.15 . . 2 . . . . . . . . 6485 1 144 . 1 1 10 10 A H5'' H 1 4.52 . . 2 . . . . . . . . 6485 1 145 . 1 1 10 10 A C1' C 13 92.6 . . 1 . . . . . . . . 6485 1 146 . 1 1 10 10 A C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 147 . 1 1 10 10 A C3' C 13 73.3 . . 1 . . . . . . . . 6485 1 148 . 1 1 10 10 A C4' C 13 82.6 . . 1 . . . . . . . . 6485 1 149 . 1 1 10 10 A C5' C 13 65.7 . . 1 . . . . . . . . 6485 1 150 . 1 1 11 11 U H5 H 1 4.97 . . 1 . . . . . . . . 6485 1 151 . 1 1 11 11 U H6 H 1 7.34 . . 1 . . . . . . . . 6485 1 152 . 1 1 11 11 U C5 C 13 103.7 . . 1 . . . . . . . . 6485 1 153 . 1 1 11 11 U C6 C 13 140.7 . . 1 . . . . . . . . 6485 1 154 . 1 1 11 11 U H1' H 1 5.49 . . 1 . . . . . . . . 6485 1 155 . 1 1 11 11 U H2' H 1 4.37 . . 1 . . . . . . . . 6485 1 156 . 1 1 11 11 U H3' H 1 4.34 . . 1 . . . . . . . . 6485 1 157 . 1 1 11 11 U H4' H 1 4.37 . . 1 . . . . . . . . 6485 1 158 . 1 1 11 11 U H5' H 1 4.09 . . 2 . . . . . . . . 6485 1 159 . 1 1 11 11 U H5'' H 1 4.44 . . 2 . . . . . . . . 6485 1 160 . 1 1 11 11 U C1' C 13 93.3 . . 1 . . . . . . . . 6485 1 161 . 1 1 11 11 U C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 162 . 1 1 11 11 U C3' C 13 72.9 . . 1 . . . . . . . . 6485 1 163 . 1 1 11 11 U C4' C 13 82.5 . . 1 . . . . . . . . 6485 1 164 . 1 1 11 11 U C5' C 13 65.3 . . 1 . . . . . . . . 6485 1 165 . 1 1 12 12 G H8 H 1 7.79 . . 1 . . . . . . . . 6485 1 166 . 1 1 12 12 G C8 C 13 137.4 . . 1 . . . . . . . . 6485 1 167 . 1 1 12 12 G H1' H 1 5.55 . . 1 . . . . . . . . 6485 1 168 . 1 1 12 12 G H2' H 1 4.30 . . 1 . . . . . . . . 6485 1 169 . 1 1 12 12 G H3' H 1 4.59 . . 1 . . . . . . . . 6485 1 170 . 1 1 12 12 G H4' H 1 4.42 . . 1 . . . . . . . . 6485 1 171 . 1 1 12 12 G H5' H 1 4.10 . . 2 . . . . . . . . 6485 1 172 . 1 1 12 12 G H5'' H 1 4.34 . . 2 . . . . . . . . 6485 1 173 . 1 1 12 12 G C1' C 13 91.9 . . 1 . . . . . . . . 6485 1 174 . 1 1 12 12 G C2' C 13 76.0 . . 1 . . . . . . . . 6485 1 175 . 1 1 12 12 G C3' C 13 74.5 . . 1 . . . . . . . . 6485 1 176 . 1 1 12 12 G C4' C 13 83.5 . . 1 . . . . . . . . 6485 1 177 . 1 1 12 12 G C5' C 13 66.0 . . 1 . . . . . . . . 6485 1 178 . 1 1 13 13 C H5 H 1 5.62 . . 1 . . . . . . . . 6485 1 179 . 1 1 13 13 C H6 H 1 7.52 . . 1 . . . . . . . . 6485 1 180 . 1 1 13 13 C C5 C 13 97.9 . . 1 . . . . . . . . 6485 1 181 . 1 1 13 13 C C6 C 13 143.7 . . 1 . . . . . . . . 6485 1 182 . 1 1 13 13 C H1' H 1 5.15 . . 1 . . . . . . . . 6485 1 183 . 1 1 13 13 C H2' H 1 4.32 . . 1 . . . . . . . . 6485 1 184 . 1 1 13 13 C H3' H 1 4.17 . . 1 . . . . . . . . 6485 1 185 . 1 1 13 13 C H4' H 1 4.10 . . 1 . . . . . . . . 6485 1 186 . 1 1 13 13 C H5' H 1 3.97 . . 2 . . . . . . . . 6485 1 187 . 1 1 13 13 C H5'' H 1 4.16 . . 2 . . . . . . . . 6485 1 188 . 1 1 13 13 C C1' C 13 92.4 . . 1 . . . . . . . . 6485 1 189 . 1 1 13 13 C C2' C 13 75.4 . . 1 . . . . . . . . 6485 1 190 . 1 1 13 13 C C3' C 13 75.4 . . 1 . . . . . . . . 6485 1 191 . 1 1 13 13 C C4' C 13 84.1 . . 1 . . . . . . . . 6485 1 192 . 1 1 13 13 C C5' C 13 66.7 . . 1 . . . . . . . . 6485 1 193 . 1 1 14 14 U H5 H 1 5.76 . . 1 . . . . . . . . 6485 1 194 . 1 1 14 14 U H6 H 1 7.70 . . 1 . . . . . . . . 6485 1 195 . 1 1 14 14 U C5 C 13 105.3 . . 1 . . . . . . . . 6485 1 196 . 1 1 14 14 U C6 C 13 143.7 . . 1 . . . . . . . . 6485 1 197 . 1 1 14 14 U H1' H 1 5.66 . . 1 . . . . . . . . 6485 1 198 . 1 1 14 14 U H2' H 1 4.29 . . 1 . . . . . . . . 6485 1 199 . 1 1 14 14 U H3' H 1 4.41 . . 1 . . . . . . . . 6485 1 200 . 1 1 14 14 U H4' H 1 4.18 . . 1 . . . . . . . . 6485 1 201 . 1 1 14 14 U H5' H 1 3.88 . . 2 . . . . . . . . 6485 1 202 . 1 1 14 14 U H5'' H 1 3.94 . . 2 . . . . . . . . 6485 1 203 . 1 1 14 14 U C1' C 13 91.3 . . 1 . . . . . . . . 6485 1 204 . 1 1 14 14 U C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 205 . 1 1 14 14 U C3' C 13 75.5 . . 1 . . . . . . . . 6485 1 206 . 1 1 14 14 U C4' C 13 84.6 . . 1 . . . . . . . . 6485 1 207 . 1 1 14 14 U C5' C 13 66.5 . . 1 . . . . . . . . 6485 1 208 . 1 1 15 15 A H2 H 1 8.01 . . 1 . . . . . . . . 6485 1 209 . 1 1 15 15 A H8 H 1 8.08 . . 1 . . . . . . . . 6485 1 210 . 1 1 15 15 A C2 C 13 155 . . 1 . . . . . . . . 6485 1 211 . 1 1 15 15 A C8 C 13 141.9 . . 1 . . . . . . . . 6485 1 212 . 1 1 15 15 A H1' H 1 5.84 . . 1 . . . . . . . . 6485 1 213 . 1 1 15 15 A H2' H 1 4.75 . . 1 . . . . . . . . 6485 1 214 . 1 1 15 15 A H3' H 1 4.41 . . 1 . . . . . . . . 6485 1 215 . 1 1 15 15 A H4' H 1 4.38 . . 1 . . . . . . . . 6485 1 216 . 1 1 15 15 A H5' H 1 3.99 . . 2 . . . . . . . . 6485 1 217 . 1 1 15 15 A H5'' H 1 4.15 . . 2 . . . . . . . . 6485 1 218 . 1 1 15 15 A C1' C 13 91.7 . . 1 . . . . . . . . 6485 1 219 . 1 1 15 15 A C2' C 13 75.7 . . 1 . . . . . . . . 6485 1 220 . 1 1 15 15 A C3' C 13 72.7 . . 1 . . . . . . . . 6485 1 221 . 1 1 15 15 A C4' C 13 84.2 . . 1 . . . . . . . . 6485 1 222 . 1 1 15 15 A C5' C 13 67.1 . . 1 . . . . . . . . 6485 1 223 . 1 1 16 16 A H2 H 1 8.10 . . 1 . . . . . . . . 6485 1 224 . 1 1 16 16 A H8 H 1 8.08 . . 1 . . . . . . . . 6485 1 225 . 1 1 16 16 A C2 C 13 155.2 . . 1 . . . . . . . . 6485 1 226 . 1 1 16 16 A C8 C 13 141.7 . . 1 . . . . . . . . 6485 1 227 . 1 1 16 16 A H1' H 1 5.59 . . 1 . . . . . . . . 6485 1 228 . 1 1 16 16 A H2' H 1 4.74 . . 1 . . . . . . . . 6485 1 229 . 1 1 16 16 A H3' H 1 4.39 . . 1 . . . . . . . . 6485 1 230 . 1 1 16 16 A H4' H 1 4.54 . . 1 . . . . . . . . 6485 1 231 . 1 1 16 16 A H5' H 1 4.31 . . 2 . . . . . . . . 6485 1 232 . 1 1 16 16 A H5'' H 1 4.37 . . 2 . . . . . . . . 6485 1 233 . 1 1 16 16 A C1' C 13 91.6 . . 1 . . . . . . . . 6485 1 234 . 1 1 16 16 A C2' C 13 75.9 . . 1 . . . . . . . . 6485 1 235 . 1 1 16 16 A C3' C 13 74.3 . . 1 . . . . . . . . 6485 1 236 . 1 1 16 16 A C4' C 13 83.8 . . 1 . . . . . . . . 6485 1 237 . 1 1 16 16 A C5' C 13 67.9 . . 1 . . . . . . . . 6485 1 238 . 1 1 17 17 A H2 H 1 7.87 . . 1 . . . . . . . . 6485 1 239 . 1 1 17 17 A H8 H 1 8.15 . . 1 . . . . . . . . 6485 1 240 . 1 1 17 17 A C2 C 13 154.1 . . 1 . . . . . . . . 6485 1 241 . 1 1 17 17 A C8 C 13 140.7 . . 1 . . . . . . . . 6485 1 242 . 1 1 17 17 A H1' H 1 5.01 . . 1 . . . . . . . . 6485 1 243 . 1 1 17 17 A H2' H 1 4.41 . . 1 . . . . . . . . 6485 1 244 . 1 1 17 17 A H3' H 1 4.4 . . 1 . . . . . . . . 6485 1 245 . 1 1 17 17 A H4' H 1 4.39 . . 1 . . . . . . . . 6485 1 246 . 1 1 17 17 A H5' H 1 4.28 . . 2 . . . . . . . . 6485 1 247 . 1 1 17 17 A H5'' H 1 4.33 . . 2 . . . . . . . . 6485 1 248 . 1 1 17 17 A C1' C 13 93.0 . . 1 . . . . . . . . 6485 1 249 . 1 1 17 17 A C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 250 . 1 1 17 17 A C3' C 13 74.2 . . 1 . . . . . . . . 6485 1 251 . 1 1 17 17 A C4' C 13 83.0 . . 1 . . . . . . . . 6485 1 252 . 1 1 17 17 A C5' C 13 67.6 . . 1 . . . . . . . . 6485 1 253 . 1 1 18 18 U H3 H 1 13.62 . . 1 . . . . . . . . 6485 1 254 . 1 1 18 18 U H5 H 1 5.11 . . 1 . . . . . . . . 6485 1 255 . 1 1 18 18 U H6 H 1 7.53 . . 1 . . . . . . . . 6485 1 256 . 1 1 18 18 U C5 C 13 103.3 . . 1 . . . . . . . . 6485 1 257 . 1 1 18 18 U C6 C 13 141.8 . . 1 . . . . . . . . 6485 1 258 . 1 1 18 18 U H1' H 1 5.57 . . 1 . . . . . . . . 6485 1 259 . 1 1 18 18 U H2' H 1 4.52 . . 1 . . . . . . . . 6485 1 260 . 1 1 18 18 U H3' H 1 4.47 . . 1 . . . . . . . . 6485 1 261 . 1 1 18 18 U H4' H 1 4.41 . . 1 . . . . . . . . 6485 1 262 . 1 1 18 18 U H5' H 1 4.08 . . 2 . . . . . . . . 6485 1 263 . 1 1 18 18 U H5'' H 1 4.43 . . 2 . . . . . . . . 6485 1 264 . 1 1 18 18 U C1' C 13 92.82 . . 1 . . . . . . . . 6485 1 265 . 1 1 18 18 U C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 266 . 1 1 18 18 U C3' C 13 73.3 . . 1 . . . . . . . . 6485 1 267 . 1 1 18 18 U C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 268 . 1 1 18 18 U C5' C 13 65.1 . . 1 . . . . . . . . 6485 1 269 . 1 1 19 19 G H1 H 1 11 . . 1 . . . . . . . . 6485 1 270 . 1 1 19 19 G H8 H 1 7.67 . . 1 . . . . . . . . 6485 1 271 . 1 1 19 19 G C8 C 13 137.4 . . 1 . . . . . . . . 6485 1 272 . 1 1 19 19 G H1' H 1 5.77 . . 1 . . . . . . . . 6485 1 273 . 1 1 19 19 G H2' H 1 4.63 . . 1 . . . . . . . . 6485 1 274 . 1 1 19 19 G H3' H 1 4.25 . . 1 . . . . . . . . 6485 1 275 . 1 1 19 19 G H4' H 1 4.52 . . 1 . . . . . . . . 6485 1 276 . 1 1 19 19 G H5' H 1 4.15 . . 2 . . . . . . . . 6485 1 277 . 1 1 19 19 G H5'' H 1 4.39 . . 2 . . . . . . . . 6485 1 278 . 1 1 19 19 G C1' C 13 93.7 . . 1 . . . . . . . . 6485 1 279 . 1 1 19 19 G C2' C 13 75.3 . . 1 . . . . . . . . 6485 1 280 . 1 1 19 19 G C3' C 13 73.6 . . 1 . . . . . . . . 6485 1 281 . 1 1 19 19 G C4' C 13 82.5 . . 1 . . . . . . . . 6485 1 282 . 1 1 19 19 G C5' C 13 67.2 . . 1 . . . . . . . . 6485 1 283 . 1 1 20 20 U H3 H 1 14.2 . . 1 . . . . . . . . 6485 1 284 . 1 1 20 20 U H5 H 1 5.16 . . 1 . . . . . . . . 6485 1 285 . 1 1 20 20 U H6 H 1 7.62 . . 1 . . . . . . . . 6485 1 286 . 1 1 20 20 U C5 C 13 103.2 . . 1 . . . . . . . . 6485 1 287 . 1 1 20 20 U C6 C 13 141.1 . . 1 . . . . . . . . 6485 1 288 . 1 1 20 20 U H1' H 1 5.42 . . 1 . . . . . . . . 6485 1 289 . 1 1 20 20 U H2' H 1 4.35 . . 1 . . . . . . . . 6485 1 290 . 1 1 20 20 U H3' H 1 4.46 . . 1 . . . . . . . . 6485 1 291 . 1 1 20 20 U H4' H 1 4.41 . . 1 . . . . . . . . 6485 1 292 . 1 1 20 20 U H5' H 1 4.08 . . 2 . . . . . . . . 6485 1 293 . 1 1 20 20 U H5'' H 1 4.5 . . 2 . . . . . . . . 6485 1 294 . 1 1 20 20 U C1' C 13 94.1 . . 1 . . . . . . . . 6485 1 295 . 1 1 20 20 U C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 296 . 1 1 20 20 U C3' C 13 72.1 . . 1 . . . . . . . . 6485 1 297 . 1 1 20 20 U C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 298 . 1 1 20 20 U C5' C 13 64.1 . . 1 . . . . . . . . 6485 1 299 . 1 1 21 21 U H3 H 1 13.21 . . 1 . . . . . . . . 6485 1 300 . 1 1 21 21 U H5 H 1 5.53 . . 1 . . . . . . . . 6485 1 301 . 1 1 21 21 U H6 H 1 7.88 . . 1 . . . . . . . . 6485 1 302 . 1 1 21 21 U C5 C 13 103.9 . . 1 . . . . . . . . 6485 1 303 . 1 1 21 21 U C6 C 13 142.0 . . 1 . . . . . . . . 6485 1 304 . 1 1 21 21 U H1' H 1 5.59 . . 1 . . . . . . . . 6485 1 305 . 1 1 21 21 U H2' H 1 4.64 . . 1 . . . . . . . . 6485 1 306 . 1 1 21 21 U H3' H 1 4.57 . . 1 . . . . . . . . 6485 1 307 . 1 1 21 21 U H4' H 1 4.46 . . 1 . . . . . . . . 6485 1 308 . 1 1 21 21 U H5' H 1 4.12 . . 2 . . . . . . . . 6485 1 309 . 1 1 21 21 U H5'' H 1 4.51 . . 2 . . . . . . . . 6485 1 310 . 1 1 21 21 U C1' C 13 93.6 . . 1 . . . . . . . . 6485 1 311 . 1 1 21 21 U C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 312 . 1 1 21 21 U C3' C 13 73.0 . . 1 . . . . . . . . 6485 1 313 . 1 1 21 21 U C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 314 . 1 1 21 21 U C5' C 13 65.0 . . 1 . . . . . . . . 6485 1 315 . 1 1 22 22 G H1 H 1 12.48 . . 1 . . . . . . . . 6485 1 316 . 1 1 22 22 G H8 H 1 7.69 . . 1 . . . . . . . . 6485 1 317 . 1 1 22 22 G C8 C 13 136.7 . . 1 . . . . . . . . 6485 1 318 . 1 1 22 22 G H1' H 1 5.71 . . 1 . . . . . . . . 6485 1 319 . 1 1 22 22 G H2' H 1 4.48 . . 1 . . . . . . . . 6485 1 320 . 1 1 22 22 G H3' H 1 4.51 . . 1 . . . . . . . . 6485 1 321 . 1 1 22 22 G H4' H 1 4.52 . . 1 . . . . . . . . 6485 1 322 . 1 1 22 22 G H5' H 1 4.16 . . 2 . . . . . . . . 6485 1 323 . 1 1 22 22 G H5'' H 1 4.48 . . 2 . . . . . . . . 6485 1 324 . 1 1 22 22 G C1' C 13 93.1 . . 1 . . . . . . . . 6485 1 325 . 1 1 22 22 G C2' C 13 75.3 . . 1 . . . . . . . . 6485 1 326 . 1 1 22 22 G C3' C 13 73.4 . . 1 . . . . . . . . 6485 1 327 . 1 1 22 22 G C4' C 13 82.5 . . 1 . . . . . . . . 6485 1 328 . 1 1 22 22 G C5' C 13 66.2 . . 1 . . . . . . . . 6485 1 329 . 1 1 23 23 U H3 H 1 14.25 . . 1 . . . . . . . . 6485 1 330 . 1 1 23 23 U H5 H 1 5.02 . . 1 . . . . . . . . 6485 1 331 . 1 1 23 23 U H6 H 1 7.77 . . 1 . . . . . . . . 6485 1 332 . 1 1 23 23 U C5 C 13 102.6 . . 1 . . . . . . . . 6485 1 333 . 1 1 23 23 U C6 C 13 142 . . 1 . . . . . . . . 6485 1 334 . 1 1 23 23 U H1' H 1 5.46 . . 1 . . . . . . . . 6485 1 335 . 1 1 23 23 U H2' H 1 4.41 . . 1 . . . . . . . . 6485 1 336 . 1 1 23 23 U H3' H 1 4.46 . . 1 . . . . . . . . 6485 1 337 . 1 1 23 23 U H4' H 1 4.44 . . 1 . . . . . . . . 6485 1 338 . 1 1 23 23 U H5' H 1 4.10 . . 2 . . . . . . . . 6485 1 339 . 1 1 23 23 U H5'' H 1 4.57 . . 2 . . . . . . . . 6485 1 340 . 1 1 23 23 U C1' C 13 94.0 . . 1 . . . . . . . . 6485 1 341 . 1 1 23 23 U C2' C 13 75.3 . . 1 . . . . . . . . 6485 1 342 . 1 1 23 23 U C3' C 13 72.2 . . 1 . . . . . . . . 6485 1 343 . 1 1 23 23 U C4' C 13 82.3 . . 1 . . . . . . . . 6485 1 344 . 1 1 23 23 U C5' C 13 64.5 . . 1 . . . . . . . . 6485 1 345 . 1 1 24 24 U H3 H 1 13.12 . . 1 . . . . . . . . 6485 1 346 . 1 1 24 24 U H5 H 1 5.59 . . 1 . . . . . . . . 6485 1 347 . 1 1 24 24 U H6 H 1 7.99 . . 1 . . . . . . . . 6485 1 348 . 1 1 24 24 U C5 C 13 103.7 . . 1 . . . . . . . . 6485 1 349 . 1 1 24 24 U C6 C 13 142.3 . . 1 . . . . . . . . 6485 1 350 . 1 1 24 24 U H1' H 1 5.59 . . 1 . . . . . . . . 6485 1 351 . 1 1 24 24 U H2' H 1 4.48 . . 1 . . . . . . . . 6485 1 352 . 1 1 24 24 U H3' H 1 4.61 . . 1 . . . . . . . . 6485 1 353 . 1 1 24 24 U H4' H 1 4.45 . . 1 . . . . . . . . 6485 1 354 . 1 1 24 24 U H5' H 1 4.13 . . 2 . . . . . . . . 6485 1 355 . 1 1 24 24 U H5'' H 1 4.54 . . 2 . . . . . . . . 6485 1 356 . 1 1 24 24 U C1' C 13 93.6 . . 1 . . . . . . . . 6485 1 357 . 1 1 24 24 U C2' C 13 75.5 . . 1 . . . . . . . . 6485 1 358 . 1 1 24 24 U C3' C 13 72.6 . . 1 . . . . . . . . 6485 1 359 . 1 1 24 24 U C4' C 13 82.2 . . 1 . . . . . . . . 6485 1 360 . 1 1 24 24 U C5' C 13 64.8 . . 1 . . . . . . . . 6485 1 361 . 1 1 25 25 A H2 H 1 7.04 . . 1 . . . . . . . . 6485 1 362 . 1 1 25 25 A H8 H 1 8.19 . . 1 . . . . . . . . 6485 1 363 . 1 1 25 25 A C2 C 13 153.5 . . 1 . . . . . . . . 6485 1 364 . 1 1 25 25 A C8 C 13 139.8 . . 1 . . . . . . . . 6485 1 365 . 1 1 25 25 A H1' H 1 5.96 . . 1 . . . . . . . . 6485 1 366 . 1 1 25 25 A H2' H 1 4.46 . . 1 . . . . . . . . 6485 1 367 . 1 1 25 25 A H3' H 1 4.68 . . 1 . . . . . . . . 6485 1 368 . 1 1 25 25 A H4' H 1 4.49 . . 1 . . . . . . . . 6485 1 369 . 1 1 25 25 A H5' H 1 4.16 . . 2 . . . . . . . . 6485 1 370 . 1 1 25 25 A H5'' H 1 4.58 . . 2 . . . . . . . . 6485 1 371 . 1 1 25 25 A C1' C 13 93.0 . . 1 . . . . . . . . 6485 1 372 . 1 1 25 25 A C2' C 13 75.8 . . 1 . . . . . . . . 6485 1 373 . 1 1 25 25 A C3' C 13 72.9 . . 1 . . . . . . . . 6485 1 374 . 1 1 25 25 A C4' C 13 82.1 . . 1 . . . . . . . . 6485 1 375 . 1 1 25 25 A C5' C 13 65.2 . . 1 . . . . . . . . 6485 1 376 . 1 1 26 26 C H5 H 1 5.18 . . 1 . . . . . . . . 6485 1 377 . 1 1 26 26 C H6 H 1 7.51 . . 1 . . . . . . . . 6485 1 378 . 1 1 26 26 C C5 C 13 97.1 . . 1 . . . . . . . . 6485 1 379 . 1 1 26 26 C C6 C 13 140.9 . . 1 . . . . . . . . 6485 1 380 . 1 1 26 26 C H1' H 1 5.33 . . 1 . . . . . . . . 6485 1 381 . 1 1 26 26 C H2' H 1 4.04 . . 1 . . . . . . . . 6485 1 382 . 1 1 26 26 C H3' H 1 4.33 . . 1 . . . . . . . . 6485 1 383 . 1 1 26 26 C H4' H 1 4.33 . . 1 . . . . . . . . 6485 1 384 . 1 1 26 26 C H5' H 1 4.01 . . 2 . . . . . . . . 6485 1 385 . 1 1 26 26 C H5'' H 1 4.49 . . 2 . . . . . . . . 6485 1 386 . 1 1 26 26 C C1' C 13 94.0 . . 1 . . . . . . . . 6485 1 387 . 1 1 26 26 C C2' C 13 75.9 . . 1 . . . . . . . . 6485 1 388 . 1 1 26 26 C C3' C 13 72.3 . . 1 . . . . . . . . 6485 1 389 . 1 1 26 26 C C4' C 13 81.9 . . 1 . . . . . . . . 6485 1 390 . 1 1 26 26 C C5' C 13 64.7 . . 1 . . . . . . . . 6485 1 391 . 1 1 27 27 C H5 H 1 5.4 . . 1 . . . . . . . . 6485 1 392 . 1 1 27 27 C H6 H 1 7.59 . . 1 . . . . . . . . 6485 1 393 . 1 1 27 27 C C5 C 13 98.2 . . 1 . . . . . . . . 6485 1 394 . 1 1 27 27 C C6 C 13 141.9 . . 1 . . . . . . . . 6485 1 395 . 1 1 27 27 C H1' H 1 5.71 . . 1 . . . . . . . . 6485 1 396 . 1 1 27 27 C H2' H 1 3.97 . . 1 . . . . . . . . 6485 1 397 . 1 1 27 27 C H3' H 1 4.14 . . 1 . . . . . . . . 6485 1 398 . 1 1 27 27 C H4' H 1 4.12 . . 1 . . . . . . . . 6485 1 399 . 1 1 27 27 C H5' H 1 3.99 . . 2 . . . . . . . . 6485 1 400 . 1 1 27 27 C H5'' H 1 4.42 . . 2 . . . . . . . . 6485 1 401 . 1 1 27 27 C C1' C 13 93.0 . . 1 . . . . . . . . 6485 1 402 . 1 1 27 27 C C2' C 13 77.7 . . 1 . . . . . . . . 6485 1 403 . 1 1 27 27 C C3' C 13 70.0 . . 1 . . . . . . . . 6485 1 404 . 1 1 27 27 C C4' C 13 83.6 . . 1 . . . . . . . . 6485 1 405 . 1 1 27 27 C C5' C 13 65.3 . . 1 . . . . . . . . 6485 1 stop_ save_