Temperature: 298K; p1:13.45 ;# 90 degree 1H hard pulse SR:-42.88 ;# Chemical shift reference (DSS) SWH:0.5:6.0 ;# 1H SW SWC_ALL:0:220 ;# 13C SW (ALL) SWC_H:60:110 ;# 13C SW (only 13C with 1H attached) Processing log: EXPNO=1 1D-1H DONE! ******************************* Peak_list: cq_00143_1.list Spectrum_figure: cq_00143_1.pdf Parameters: sr=-42.880001 ; f1p=6.107165 ; f2p=0.607165 EXPNO=2 2D-[1H,1H]-TOCSY DONE! ******************************* Peak_list: cq_00143_2.list Spectrum_figure: cq_00143_2.pdf spectrum: cq_00143_2.ft2 Parameters: sr=-42.880001 ; f1_low=6.091121 ; f1_high=0.787481 ; f2_low=5.767724 ; f2_high=0.875708 EXPNO=3 1D-13C DONE! ******************************* Peak_list: cq_00143_3.list Spectrum_figure: cq_00143_3.pdf Parameters: sr=-239.343256 ; f1p=222.378860 ; f2p=2.378857 EXPNO=5 1D-13C-DEPT135 DONE! ******************************* Peak_list: cq_00143_5.list Spectrum_figure: cq_00143_5.pdf Parameters: sr=-239.343256 ; f1p=112.378853 ; f2p=62.378857 EXPNO=4 1D-13C-DEPT90 DONE! ******************************* Peak_list: cq_00143_4.list Spectrum_figure: cq_00143_4.pdf Parameters: sr=-239.343256 ; f1p=112.378853 ; f2p=62.378857 EXPNO=6 2D-[1H,13C]-HSQCSE DONE! ******************************* Peak_list: cq_00143_6.list Spectrum_figure: cq_00143_6.pdf spectrum: cq_00143_6.ft2 Parameters: sr=-42.880001 ; csr=-239.343256, f1_low=5.980537 ; f1_high=3.270048 ; f2_low=106.715569 ; f2_high=63.315395