Temperature: 298K; p1:13.125 ;# 90 degree 1H hard pulse SR:-37.3 ;# Chemical shift reference (DSS) SWH:0.5:5.0 ;# 1H SW SWC_ALL:0:220 ;# 13C SW (ALL) SWC_H:0:60 ;# 13C SW (only 13C with 1H attached) S/N:weak Processing log: EXPNO=1 1D-1H DONE! ******************************* Peak_list: cq_02999_1.list Spectrum_figure: cq_02999_1.pdf Parameters: sr=-37.299999 ; f1p=5.093220 ; f2p=0.593220 EXPNO=2 2D-[1H,1H]-TOCSY DONE! ******************************* Peak_list: cq_02999_2.list Spectrum_figure: cq_02999_2.pdf spectrum: cq_02999_2.ft2 Parameters: sr=-37.299999 ; f1_low=4.356869 ; f1_high=0.593220 ; f2_low=4.274086 ; f2_high=0.593220 EXPNO=3 1D-13C DONE! ******************************* Peak_list: cq_02999_3.list Spectrum_figure: cq_02999_3.pdf Parameters: sr=-237.940167 ; f1p=222.364914 ; f2p=2.364911 EXPNO=5 1D-13C-DEPT135 DONE! ******************************* Peak_list: cq_02999_5.list Spectrum_figure: cq_02999_5.pdf Parameters: sr=-237.940167 ; f1p=62.364910 ; f2p=2.364911 EXPNO=6 2D-[1H,13C]-HSQCSE DONE! ******************************* Peak_list: cq_02999_6.list Spectrum_figure: cq_02999_6.pdf spectrum: cq_02999_6.ft2 Parameters: sr=-37.299999 ; csr=-237.940167, f1_low=4.617214 ; f1_high=0.593220 ; f2_low=58.557800 ; f2_high=11.523259 EXPNO=4 1D-13C-DEPT90 DONE! ******************************* Peak_list: cq_02999_4.list Spectrum_figure: cq_02999_4.pdf Parameters: sr=-237.940167 ; f1p=62.364910 ; f2p=2.364911